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, ‘ 4 © +FD-302a (Rev. 10-6-95) bé bIc 279A-WEF-222936 Continuation of FD-302 of | | ,On 12/01/2006 ,Page_ —2- [__aia not know the original reasoning behind purchasing the Iyophilizer, but it is set up for stoppering, using vials with rubber caps. The main cha j efrigerated in order to keep samples cold. According | drying spores is a, “no-no”. [__sdjnever saw the front of the lyophilizer obscured in any way. The lyophilizer is s hat noisy, such that you would b6 notice if it were running from fbut not from the hallway. b7c Once the lyophilizer is started, it takes approximately 1 hour for the sample chamber to achieve -40 degrees Celsius. The lyophilizer would be ready in about 5 minutes if you were not interested in cooling down the sample chamber. Once the lyophilization is complete, it takes only minutes to get the samples out, however, it could take hours to thaw the cold trap depending on the volume of icé present. belongs to IVINS. escorted the interviewing agents to suite| | and started up the lyophilizer. The lyophilizer is further described as a rovided the interviewin agents with an article describing which describes a copy of the "Operational Instructions for Lyophilizer" (1 page), and the manufacturer's "Operation Summary" (1 page). These items are included in the 1A along with the original notes of the interview, the t =—mai as shown to [Jan one partial schematic witht] indication o e lyophilizer location. [| "8 glad to help, and was agreeable to re- contact by € interviewing agents.